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6
CH3041
GC I
• Analytes must be volatile. Separations rely on the volatility of the gases & their affinity for the liquid stationary phase that is supported on fused silica (tubular column).
Column types: 1) packed - column full of SP
2) capillary , open tubular column with the
walls coated with the SP.  0.3mm, 30 - 60 m
SP: Carbowax (polar perfumes)
Detectors:
i) FID Flame Ionisation Detector:oils, FAMES
ii) FPD Flame photometric: OP pesticides
iii) ECD Electron capture : OC pesticides
iv) MS Mass spectrometer: PCBs, VOCs ...